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 Transport Properties of Trifluoromethanesulfonic Acid Monohydrate. A Study of Diffusivity, Conductivity, and Viscosity
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Transport Properties of Trifluoromethanesulfonic Acid Monohydrate. A Study of Diffusivity, Conductivity, and Viscosity

автор Mohammed A. издательство Книга по Требованию Книги
Cтраниц 64        мягкая обложка       
Аннотация:NMR spectra indicate that proton diffusion occurs via direct hopping from TFMSA molecule to molecule. The conductivity of the solution was found to be in good agreement with literature values. Temperature dependences of the measured properties showed Arrhenius behavior with comparable activation energies for proton diffusion, fluorine diffusion, ionic conduction, and viscosity. Conductivities were measured using electrochemical impedance spectroscopy (EIS) on standard equipment and viscosities were determined using a Cannon-Ubbelohde viscometer. The degree of dissociation of the charged species varied from 25 to 29% over the temperature range, with an estimated dissociation energy of 2. 8+/-0. 14 kJ/mol for the TFMSA monohydrate molecule. Proton and fluorine diffusivity, ionic conductivity, and viscosity of trifluoromethanesulfonic acid (TFMSA) monohydrate have been measured over a wide range of temperatures. Protons were found to diffuse approximately 1. 5 times faster than fluorines over the entire temperature range of 40 degC to 110 degC. Diffusivities were measured using the pulsed-gradient spin-echo (PGSE) technique on a 300 MHz NMR spectrometer.
Автор: Mohammed A.
Издательство: Книга по Требованию
Год:2010
Цена:
1893 руб
Нет в наличии
Поиск: Transport Properties of Trifluoromethanesulfonic Acid Monohydrate. A Study of Diffusivity, Conductivity, and Viscosity


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